By Stefhanni J.
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The constants in this experiment were:
The way the apparatus was set up
Same atmospheric conditions
The gauge and the length of the wires was the same
The same method of attachment was used
The same temperature points
The chemicals that are being used to get to the temperatures
The same place of application
The manipulated variable in this experiment was
the types of wire being used and the temperature points at which they are
being tested. The responding variable was the weight at which the wires
break at the different temperatures.
To measure the responding variable, mass
the weight of all of the materials below where the wire was connected to
the lower portion of the apparatus. To accomplish this, place all of the
parts into the small bucket and mass them with the triple beam balance.
Also the mass of the liquids that are being used at the moment the wire
breaks should be measured. To do this you have to measure 120 ml of H2O
in the can, then mark it with a line of masking tape. Then you have to
find the density and solve the equation m=d/v to find the mass of the liquid.
According to my results the hypothesis was rejected,
but I cannot be certain because the annealed steel was inconsistent in
the results. From all three tests I concluded that the galvanized steel
was stronger than the annealed steel and all the other wires I tested.
Even though the annealed steel was inconsistent all of the results on that
wire showed that even at its highest the annealed steel wire held significantly
less than the galvanized steel wire. One question that I had during the
testing with the Liquid nitrogen was why did all of the wires break above
the liquid nitrogen.
A possible systematic error was that the liquid
nitrogen does have weight that I did not add to the weight of the tests.
The way the apparatus was set up
Same atmospheric conditions
The gauge and the length of the wires was the same
The same method of attachment was used
The same temperature points
The chemicals that are being used to get to the temperatures
The same place of application
The manipulated variable in this experiment was the types of wire
being used and the temperature points at which they are being tested. The
responding variable was the weight at which the wires break at the different
temperatures.
To measure the responding variable, mass
the weight of all of the materials below where the wire was connected to
the lower portion of the apparatus. To accomplish this, place all of the
parts into the small bucket and mass them with the triple beam balance.
Also the mass of the liquids that are being used at the moment the wire
breaks should be measured. To do this you have to measure 120 ml of HO
in the can, then mark it with a line of masking tape. Then you have to
find the density and solve the equation m=d/v to find the mass of the liquid.
For this experiment you will need:
1 Safety glasses
18 30 cm Galvanized steel Wire
18 30 cm Brass Wire
18 30 cm Steel Wire
18 30 cm Annealed Steel Wire
18 30 cm Copper Wire
1 60 centimeter 2x4 bored – 2 FT
1 Metal clamp
8 Aluminum can to hold the liquid nitrogen
1 Metal cloths hanger- straightened
10 Rubber gasket
9 Metal eyelet screws (2”)
9 Metal eyelet screws (4”)
20 Nuts
4 Washers
1 Metal piece
1 Shallow bucket with handle
1 Bottle Propane
1 Torch to use with the above fuels
2 Liters Liquid nitrogen
1 Electric drill- for metal and wood
1 Pliers
1 Wire cutters
1 Thermocouple
1 Sturdy Support- table
1 Triple beam balance
2 Sets of weights
3. Testing one of the wires for extreme heat (see figure 3)
a. Use one of the wires and wrap it around the
eyelet screw that is hanging on the hanger two times, then around the wire
itself seven times, through the hook again and around the wire three times.
b. Use 10 cm on each end for the knots at the
screws.
c. Do the same on the bottom hook (you will not
need to use the can for this experiment.)
d. Use the torch to apply heat directly under
the top screw wile adding weights to the bucket.
e. Use the Thermal Copal to verify the temperature
of the flame being applied to the wire
f. When the wire breaks, measure how much weight
is in the bucket, and add the weight of the apparatus
g. Record the weight and the temperature at which
the test wire broke.
INTRODUCTION
This
report will cover subjects of interest having to do with my project. The
following sections will include information on: the five kinds of metal
to be used in this experiment, Iron and steel manufacturing, wire making,
flames, and also information on the chemicals used to apply the different
temperatures to the wires.
MANUFACTURING
OF IRON AND STEEL
Introduction
Steel is an alloy of iron and carbon; it also contains a mixture of
other elements.
Some alloys irons contain more carbon more than steels. Open-hearth iron
and wrought iron contain only a few hundredths of one percent of carbon,
Steels contain 0.04 percent to 2.25 percent of carbon, Cast iron, malleable
cast iron, and pig iron contain between 2 to 4 percent. A group of iron
alloys, called ferroalloys, are used in the manufacturing of iron and steel
alloys; they contain 20 to 80 percent of an alloying element such as manganese,
silicon, or chromium.
Pig Iron
Production
A blast furnace consists of a cylinder steel shell lined with any nonmetallic
substance such as firebrick. The shell is narrowed at the top and at the
bottom; the widest point is about one fourth the distance from the bottom
of the shell. The bosh, the lower portion of the furnace, has several tubular
openings, called tuyeres, through which air is blasted. Close to the bottom
of the bosh is a hole where the molten pig iron flows when the furnace
is tapped, above this hole but below the tuyeres, is another hole used
to drain slag. The top of the furnace, which is about 27m high, has vents
for the gases to escape and a pair of round hoppers with bell shaped valves
through which the charge is introduced into the furnace. The materials
are brought to the hoppers in dump cars, or skips, that are hauled up an
external skip hoist. Blast furnaces operate continuously.
The unprocessed materials are separated into several small charges prior
to being fed into the furnace. They are introduces into the furnace at
10 to 15 minuet intervals. Slag is drawn from the top of the metal every
2 hours, and the iron itself is tapped about five times a day.
The air that is used to supply the blast furnace is preheated to temperature
between 540O and 870 O C. the heating is performed in stoves, which are
cylinder, containing networks of firebrick. The bricks in the stoves are
heated for several hours by burning blast furnace gas, the waste gases
from the top of the furnace. Then the flame is turned off and the air is
blown through the stove. The weight of the air used in the furnace is more
than that of the other raw materials used.
The process of tapping consists of knocking out a clay plug from the iron
hole near the bottom of the bosh and allowing the molten metal to flow
into a clay lined runner and then into a large brick lined metal container,
which may be either a ladle or a rail car capable of holding as much as
100 tons of metal. Any slag that may flow from the furnace with the metal
is skimmed off before it reaches the container. The container of molten
pig iron is then transported to the steel making shop.
Other Methods
of Iron Refining
Most of the iron and steel manufacturing in the world is made from pig
iron produced by the blast furnace process, other methods of iron refining
are possible and have been practiced to a limited extent. One method is
the ‘direct method’ of making iron and steel from ore without making pig
iron. In this process iron ore and coke are mixed in a revolving kiln and
heated to about 950 O C. carbon monoxide is given off from the heated coke
just as in the blast furnace and reduces the oxides of the ore to metallic
iron. The secondary reactions that occur in a blast furnace do not occur,
and the kiln produces ‘sponge iron’ of much higher purity than pig iron.
Pure iron also produced by electrolysis, by passing an electric current
through a solution of ferrous chloride. Neither of these processes has
achieved any great commercial significance.
Open Hearth
Process
The
making of steel from pig iron through any method consists of burning out
the leftover carbon and other impurities present in the iron. The high
melting point, about 1370 degrees Celsius, prevents the use of ordinary
fuels and furnaces. The open hearth furnace was developed to overcome this
problem; it can operate at a high temperature by regenerative preheating
the fuel gas and air used in the furnace. The exhaust gases from the furnace
are drawn through a series of chambers containing brickwork and give most
of their heat to the bricks. Then the flow is reversed and the fuel and
air pass through the heated chambers and are warmed by the bricks through
this process open hearth furnaces can reach temperatures as high as 1650
degrees Celsius.
The furnace itself consists typically of a flat, rectangular brick hearth
about 6m by 10m, which is roofed about 2.5m high. In front of the hearth
is a series of doors that open to a working floor in front of the hearth.
The entire hearth along with the working floor is one level above the ground;
the heat regenerating chambers of the furnace take up the space beneath
the hearth. A furnace this size produces about 100 metric tons of steel
every 11 hours.
The furnace is charged with cold and molten pig iron, scrap steel, and
iron oar, which supply additional oxygen; limestone is added to make the
slag more fluid. The properties of the charge vary within wide limits but
a typical charge may consist of 56,750 kg of scrap steel, 11,350 kg of
cold pig iron, 45,400 kg of molten pig iron, 11,800 kg of limestone, 900
kg of iron ore and 230 kg of fluorspar. After the furnace has been charge
it is lighted at the bottom, the operator, to provide heat regeneration,
changes the direction of the flame.
Chemically
the action of the open hearth furnace consists of lowering the carbon content
of the charge by oxidation and removing impurities such as silicon, phosphorous,
manganese, and sulfur, which combine with the limestone to make slag. This
reaction takes place while the metal in the furnace is melting, the temperature
in the furnace is held between 1540 degrees Celsius and 1650 degrees Celsius
until the molten metal has the desired carbon content. Drawing out a small
amount of molten metal from the furnace, cooling it, and then subjecting
it to physical examination or chemical analysis tests the metal.
When the carbon content is at the desired level, the furnace is tapped
through a hole at the rear of the furnace. The molten steel then flows
through a short a trough to a ladle set below the furnace at ground level.
From the ladle the steel is poured into cast iron molds that form ingots
usually 1.5 m long and 48 cm square. The raw material for all forms of
fabricated steel, these ingots weigh about 2.25 metric tons in this size.
Finishing
Processes
Steel is sold in a wide variety of sizes and shapes such as rods, pipes,
railroad rails, channels, and I-beams. These shapes are produced art steel
mills by rolling and forming heated ingots to the required shape. The work
of steel also improves the quality of the steel by refining its crystalline
structure and making the metal tougher.
The basic process of working steel is known as hot rolling. In this process
the cast ingot is heated to a bright red heat in a furnace called a soaking
pit and is then passed through a series of pairs of metal rollers that
squeeze it to the desired size and shape. The distance between the rollers
decreases for each successive pair as the steel is elongated and reduced
in thickness.
The first pair of rollers through which the ingot passes is commonly called
the blooming mill, the square billets of steel that the ingot produces
are known as blooms. From the blooming mill, the steel is passed on to
roughing mills and finally to finishing mills that reduces it to the correct
cross section. The rollers of mills used to produce railroad rails and
structural shapes such asv I-beams, H-beams, and angles are grooved to
give the required shape.
There are
five classifications of steel, they are:
Carbon Steel
Alloy Steels
High Strength Low Alloy Steels
Stainless Steels
Tool Steels
Carbon Steels make up more than 90 present of all steels, which contain
various amounts of carbon, no more than 1.65 percent manganese, 0.60 percent
silicon, and 0.60 percent copper.
Alloy steels contain certain percents of elements such as vanadium, molybdenum,
or other elements. Alloy steels contain larger amounts of other elements
(such as manganese, silicon and copper) than do regular carbon steels.
HSLA steels,
or High Strength Low Alloy Steels, are the newest of the five classifications
of steel. They are cheaper and stronger than carbon steels of the same
weight. Numerous buildings have been constructed with framework made out
of HSLA steels.
Stainless
steels contain chromium, nickel and other alloying elements that keep them
bright and rust resistant. Some of these metals are very hard and have
unusual strength and will maintain that strength for long periods of time
at extremely high and low temperatures.
Tool steels contain tungsten, melybderum and other alloying elements that
give them extra strength, hardness, and is resistant to wear.
FLAME
A flame by definition is a glowing body of mixed gasses going through the
process of combustion. Flames are a mixture of oxygen and another gas such
as hydrogen, carbon monoxide, or hydrocarbon. A typical flame is that of
a candle. When the candle is lit the heat if the match melts the wax that
is carried up the wick and then vaporized by the heat. The heat then breaks
down the vaporized wax, and combines with the oxygen of the surrounding
air, producing a flame and generating heat and light. The candle flame
consists of three zones. The innermost zone is composed of a gas air mixture
that is non luminous and is a low temperature. In the second, yellow luminous
cone, hydrogen and carbon monoxide are produced by decomposition and begin
to react with oxygen to form water and carbon dioxide. In this cone the
temperature of the flame (about 590 degrees Celsius to 680 degrees Celsius)
is great enough to detach the gasses in the flame and produce free particles
of carbon, which are to incandescence and then consumed. In the incandescent
cone the remaining carbon monoxide and hydrogen are consumed.
If a cold object is passed through the outer portions of the flame the
temperature of that part of the flame will be lowered below the point of
combustion, and the unburned carbon and carbon monoxide will be given off.
So if a porcelain dish is passed through the flame it will leave behind
a residue in the form of soot. Operation of any kind of flame producing
stove in a room that is dangerous because of the production of carbon monoxide,
which is poisonous.
All combustible substance requires specific amount of oxygen for complete
burning. (A flame can continue in an atmosphere of pure chlorine, though
combustion is not complete.) In the burning of the candle, or of solids
such as wood or coal, this oxygen is supplied by the surrounding atmosphere.
In blowpipes and various types of gas burners, air or pure oxygen is mixed
with the gas at the base of the burner so that the carbon is consumed almost
instantaneously at the mouth of the burner.
Pictures
This is a magnified picture of the copper wire after testing it
for heat
This is a magnified picture of the Annealed Steel wire after testing
it for heat
This is the apparatus for the heat testing
Table 1
Room Temperature (23 degrees C)
Metal Copper Brass
Steel Annealed Steel Galvanized
Steel
Test 1 2,400
3,000 3,200
4,800
5,400
Test 2 2,200
3,100 3,200
4,800
5,400
Test 3 2,400
3,000 3,200
4,800
5,300
Average 2,300 3,000
3,200 4,800
5,400
Table 2
Liquid Nitrogen (-195.8 degrees C)
Metal Copper Brass
Steel Annealed Steel* Galvanized
Steel
Test 1 2,500
3,000 3,500
5,000
5,500
Test 2 2,500
2,900 3,000
3,700
4,700
Test 3 2,500
2,950 3,200
4,700
5,200
Average 2,500 2,950
3,200 4,500*
5,100
Table 3
Propane (800 degrees C)
Metal Copper Brass
Steel Annealed Steel* Galvanized
Steel
Test 1 0
0 97
95
170
Test 2 0
0 99
160
170
Test 3 0
0 95
140
170
Average 0
0 97
132*
170
Table 4
All Averages
Metal Copper Brass
Steel Annealed Steel* Galvanized
Steel
195.8 C 2500
2950 3500
4500
5100
23 C 2300
3000 3200
4800
5400
800 C 0 0 97 132 170
*I was not able to make a conclusion on this wire because of
its inconsistency
All tests are calculated with out adding the weight of the apparatus except for the copper and brass in the heat test.
Bibliography
“Acetylene”
Funk & Wagnalls New Encyclopedia, 1980
“Annealing” Complete reference Library (Mindscape®), 1995
“Annealing,” Microsoft Encarta Encyclopedia, 2000
“Brass (alloy),” Microsoft Encarta Encyclopedia, 2000
“Brass” Complete reference Library (Mindscape®), 1995
“Brass” Funk & Wagnalls New Encyclopedia, 1980
“Carbon Dioxide” Complete reference Library (Mindscape®), 1995
“Carbon Dioxide” Funk & Wagnalls New Encyclopedia, 1980
“Copper” Complete reference Library (Mindscape®), 1995
“ Copper” Funk & Wagnalls New Encyclopedia, 1980
“Copper (element),” Microsoft Encarta Encyclopedia, 2000
“Flame” Complete reference Library (Mindscape®), 1995
“Flame,” Microsoft Encarta Encyclopedia, 2000
“Flame” Funk & Wagnalls New Encyclopedia, 1980
“Galvanize” Complete reference Library (Mindscape®), 1995
“Galvanized Iron” Funk & Wagnalls New Encyclopedia, 1980
“Galvanizing” Complete reference Library (Mindscape®), 1995
“Galvanizing,” Microsoft Encarta Encyclopedia, 2000
“Iron and Steel Manufacture” Funk & Wagnalls New Encyclopedia, 1980
“Iron and Steel” The World Book Encyclopedia, 1997
“Iron and Steel Manufacture,” Microsoft Encarta Encyclopedia, 2000
“Methane” Funk & Wagnalls New Encyclopedia, 1980
“Propane” Funk & Wagnalls New Encyclopedia, 1980
“Steel” Complete reference Library (Mindscape®), 1995
“Wire” Funk & Wagnalls New Encyclopedia, 1980